Please prepare your samples in the designated area or under a hood, and not on top of the magnet. The chemical shifts (d) of solvent signals observed for 1 H NMR and 13 C NMR spectra are listed in the ...

Unfortunately, many 1H-NMR spectra are severely overlapped due to the multiplet structure caused by homo-nuclear scalar couplings. "Pure shift" NMR spectra, also known as broadband homonuclear ...

Example format for compound characterisation data: mp: 100–102 °C (lit.ref 99–101 °C); [α]D = -21.5 (0.1 M in n-hexane); 1H NMR ... range of chemical shifts scanned. Specific NMR ...